ASTM D2603 - Sonic Shear Stability of Polymer-Containing Oils

Significance and Use

4.1 This test method permits the evaluation of shear stability with minimum interference from thermal and oxidative factors which may be present in some applications. Within the limitations expressed in the scope of this test method, it has been successfully applied to hydraulic fluids, transmission fluids, tractor fluids, and other fluids of similar applications. It has been found applicable to fluids containing both readily sheared and shear-resistant polymers. Correlation with perfor-mance in the case of automotive engine applications has, to date, not been established.

Scope

1.1 This test method covers the evaluation of the shear stability of an oil containing polymer in terms of the permanent loss in viscosity that results from irradiating a sample of the oil in a sonic oscillator. This test method can be useful in predicting the continuity of this property in an oil where no change is made in the base stock or the polymer. It is not intended that this test method serve to predict the performance of polymer-containing oils in service.

1.2 Evidence has been presented that correlation between the shear degradation results obtained by means of sonic oscillation and those obtained in mechanical devices can be poor. This is especially true in the case of automotive engines. Further evidence indicates that the sonic technique may rate different families of polymers in a different order than mechanical devices.

1.3 Because of these limitations, the committee under whose jurisdiction this test method falls has developed alter-native shear test methods using a diesel injector nozzle, Test Methods D5275, D6278, and D7109. While those test methods have found some utility in the evaluation of crankcase oils, the stress imparted to the sample has been found to be insufficient to shear polymers of the shear-resistant type found in aircraft hydraulic fluids.

1.4 This test method is used for polymeric additive specifications, especially in the hydraulic fluid market.

1.5 The values stated in SI units are to be regarded as standard. The values given in parentheses after SI units are provided for information only and are not considered standard.

Extracted, with permission, from ASTM D2603-20 - Sonic Shear Stability of Polymer-Containing Oils, copyright ASTM International, 100 Barr Harbor Drive, West Conshohocken, PA 19428. A copy of the complete standard may be purchased from ASTM International, astm.org